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SM ISO690:2012 CHUMAKOV, Yurii, TSAPKOV, Victor I., ANTOSYAK, Boris, SIMONOV, Yurii A., IANELLI, Sandra, BAIRAK, N., GULYA, Aurelian, PALOMARES-SÁNCHEZ, S.. Crystal structures of 2-formyl-6-methyl- and 6-bromo-2-formylpyridine 4-phenylthiosemicarbazones. In: Crystallography Reports, 2011, vol. 56, pp. 136-140. ISSN 1063-7745. DOI: https://doi.org/10.1134/S1063774510061033 |
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Crystallography Reports | |
Volumul 56 / 2011 / ISSN 1063-7745 /ISSNe 1562-689X | |
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DOI:https://doi.org/10.1134/S1063774510061033 | |
Pag. 136-140 | |
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Rezumat | |
New thiosemicarbazones-2-formyl-6-methylpyridine 4-phenylthiosemicarbazone (I) and 6-bromo-2-formylpyridine 4-phenylthiosemicarbazone hydrate (II)-were synthesized and their structures were determined. Molecules I and II are nonplanar, the phenyl moiety at the terminal nitrogen atom being rotated by 19.9° and 39.5°, respectively. The water molecule is the main factor determining the crystal packing of molecules II. |
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Cuvinte-cheie Crystal packings, Methylpyridine, Phenyl moieties, Terminal-nitrogen, Thiosemicarbazones, Water molecule |
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