Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde

Pulya A. V.; Seifullina Inna; Skorokhod L. S.; Pavlovsky Victor; Kravtsov Victor; Bogza Sergei L.; Suikov Su Yu

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PULYA, A. V., SEIFULLINA, Inna, SKOROKHOD, L. S., PAVLOVSKY, Victor, KRAVTSOV, Victor, BOGZA, Sergei L., SUIKOV, Su Yu. Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde. In: Journal of Structural Chemistry, 2018, nr. 2(59), pp. 497-501. ISSN 0022-4766. DOI: https://doi.org/10.1134/S002247661802035X

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Journal of Structural Chemistry

Numărul 2(59) / 2018 / ISSN 0022-4766

Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde

DOI:https://doi.org/10.1134/S002247661802035X

Pag. 497-501

Pulya A. V.¹, Seifullina Inna¹, Skorokhod L. S.¹, Pavlovsky Victor², Kravtsov Victor³, Bogza Sergei L.⁴, Suikov Su Yu⁴

¹ Odesa I.I.Mechnikov National University,
² A.V. Bogatsky Physico-Chemical Institute of the NAS of Ukraine,
³ Institute of Applied Physics, Academy of Sciences of Moldova,
⁴ L. M. Litvinenko Institute of Physical-Organic Chemistry and Coal Chemistry

Disponibil în IBN: 21 iunie 2018

Rezumat

Hydrazone [HydrHSal]∙Н₂О is synthesized for the first time by the interaction of 2-(7-bromo-2-oxo-5- phenyl-3H-1,4-benzdiazepin-1-yl)acetohydrazide (gidazepam) with salicylic aldehyde and characterized by the elemental analysis, thermogravimetry, mass, electron, IR, and NMR spectroscopic techniques. The molecular and crystal structure is determined by single crystal X-ray diffraction.

Cuvinte-cheie
2-(7-bromo-2-oxo-5-phenyl-3H-1,4-benzdiazepin-1-yl)acetohydrazide, gidazepam, hydrazone, salicylic aldehyde,

molecular structure, single crystal X-ray diffraction analysis

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<dc:creator>Pulya, A.</dc:creator>
<dc:creator>Seifulina, I.</dc:creator>
<dc:creator>Skorokhod, L.</dc:creator>
<dc:creator>Pavlovsky, V.I.</dc:creator>
<dc:creator>Kravţov, V.H.</dc:creator>
<dc:creator>Bogza, S.</dc:creator>
<dc:creator>Suikov, S.</dc:creator>
<dc:date>2018-03-01</dc:date>
<dc:description xml:lang='en'><p>Hydrazone [HydrHSal]∙Н<sub>2</sub>О is synthesized for the first time by the interaction of 2-(7-bromo-2-oxo-5- phenyl-3H-1,4-benzdiazepin-1-yl)acetohydrazide (gidazepam) with salicylic aldehyde and characterized by the elemental analysis, thermogravimetry, mass, electron, IR, and NMR spectroscopic techniques. The molecular and crystal structure is determined by single crystal X-ray diffraction.</p></dc:description>
<dc:identifier>10.1134/S002247661802035X</dc:identifier>
<dc:source>Journal of Structural Chemistry 59 (2) 497-501</dc:source>
<dc:subject>2-(7-bromo-2-oxo-5-phenyl-3H-1,4-benzdiazepin-1-yl)acetohydrazide</dc:subject>
<dc:subject>gidazepam</dc:subject>
<dc:subject>hydrazone</dc:subject>
<dc:subject>molecular structure</dc:subject>
<dc:subject>salicylic aldehyde</dc:subject>
<dc:subject>single crystal X-ray diffraction analysis</dc:subject>
<dc:title>Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde</dc:title>
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