Characterization of structure and luminescence of titania nanotubes
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ENACHI, Mihail; TROFIM, Viorel; TIGHINEANU, Ion; URSACHI, Veaceslav; COSEAC, Valeriu. Characterization of structure and luminescence of titania nanotubes . In: Moldavian Journal of the Physical Sciences. 2009, nr. 2(8), pp. 214-220. ISSN 1810-648X.
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Moldavian Journal of the Physical Sciences
Numărul 2(8) / 2009 / ISSN 1810-648X /ISSNe 2537-6365

Characterization of structure and luminescence of titania nanotubes

Pag. 214-220

Enachi Mihail1, Trofim Viorel1, Tighineanu Ion2, Ursachi Veaceslav2, Coseac Valeriu3
 
1 Universitatea Tehnică a Moldovei,
2 Institutul de Fizică Aplicată al AŞM,
3 Academia de Transporturi, Informatică şi Comunicaţii
 
Disponibil în IBN: 13 decembrie 2013


Rezumat

The morphology, structural, and optical properties of porous titania layers prepared by electrochemical oxidation of Ti foils are studied as a function of technological conditions of preparation and post-electrochemical-oxidation thermal treatment. Ti foils were anodized in aqueous and non-aqueous HF and H PO solutions by applying various anodizing conditions. Titania nanotubes with diameters ranging from 30 nm to 250 nm with controlled length have been prepared. The influence of thermal treatment upon the structural properties of TiO nanotubes was investigated by means of X-ray diffraction analysis and Raman scattering. It was found that the as prepared samples are amorphous. As the annealing temperature increases to 300°C, an anatase structure is formed. Starting from 500°C, a rutile structure is produced which coexists with the anatase structure. A complete phase transition to the rutile structure occurs at 800°C. The luminescence from both anatase and rutile phases was observed at low temperatures. The origin of luminescence bands is discussed.