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SM ISO690:2012 GARCIA, Carlos J., ZHUKOV, Arcady, GONZÁLEZ ESTEVEZ, Julián Maria, ZHUKOVA, V., VARGA, Rastislav, DEL VAL, Juan Jose, LARIN, Vladimir, BLANCO, Juan Maria. Studies of structural and magnetic properties of glass-coated nanocrystalline Fe79Hf7B12Si2 microwires. In: Journal of Alloys and Compounds, 2006, vol. 423, pp. 116-119. ISSN 0925-8388. DOI: https://doi.org/10.1016/j.jallcom.2005.12.029 |
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Journal of Alloys and Compounds | |
Volumul 423 / 2006 / ISSN 0925-8388 | |
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DOI:https://doi.org/10.1016/j.jallcom.2005.12.029 | |
Pag. 116-119 | |
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In the present work we deal with the fabrication of thin of Fe79Hf7B12Si2 (low Si content) glass-coated microwire with a nanocrystalline structure and structural and coercivity characterization of such samples which can be considered as a new family of these nanocrystalline materials. Pieces of 10 cm of this microwire were annealed (300-600 °C during 1 h). The structural characteristics of the as-cast and annealed samples were determined, at room temperature, by X-ray diffraction (XRD) technique. XRD measurements allow to obtain the evolution of the grain size (15-35 nm) and relative volume fraction (5-60%) of the nanograins as a function of he annealing temperature in the annealed samples. Coercive field (Hc) of the as-cast and annealed samples has been evaluated from the hysteresis loop of the samples obtained by a conventional induction method at 100 Hz. Thermal dependence Hc is quite similar to that reported in other nanocrystalline Fe-based alloys. It slightly decreases from the as-cast state (relaxation process) showing small maximum at around 700 K (pre-nucleation of nanograins) decreasing significantly between 773-873 K (exchange coupling of the nanograins). |
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Cuvinte-cheie Devitrification, Magnetic softness, Nanocrystalline alloys, Thin wires |
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