Studies of structural and magnetic properties of glass-coated nanocrystalline Fe79Hf7B12Si2 microwires
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2023-09-13 15:53
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GARCIA, Carlos J., ZHUKOV, Arcady, GONZÁLEZ ESTEVEZ, Julián Maria, ZHUKOVA, V., VARGA, Rastislav, DEL VAL, Juan Jose, LARIN, Vladimir, BLANCO, Juan Maria. Studies of structural and magnetic properties of glass-coated nanocrystalline Fe79Hf7B12Si2 microwires. In: Journal of Alloys and Compounds, 2006, vol. 423, pp. 116-119. ISSN 0925-8388. DOI: https://doi.org/10.1016/j.jallcom.2005.12.029
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Journal of Alloys and Compounds
Volumul 423 / 2006 / ISSN 0925-8388

Studies of structural and magnetic properties of glass-coated nanocrystalline Fe79Hf7B12Si2 microwires

DOI:https://doi.org/10.1016/j.jallcom.2005.12.029

Pag. 116-119

Garcia Carlos J.1, Zhukov Arcady12, González Estevez Julián Maria1, Zhukova V.3, Varga Rastislav4, del Val Juan Jose1, Larin Vladimir56, Blanco Juan Maria2
 
1 Universitatea del País Vasco UPV/EHU,
2 Universitat Politècnica de València,
3 Tamag Iberica SL,
4 Pavol Jozef Safarik University,
5 Technical University of Moldova,
6 National University of Science and Technology MISiS, Moscow
 
 
Disponibil în IBN: 6 septembrie 2023


Rezumat

In the present work we deal with the fabrication of thin of Fe79Hf7B12Si2 (low Si content) glass-coated microwire with a nanocrystalline structure and structural and coercivity characterization of such samples which can be considered as a new family of these nanocrystalline materials. Pieces of 10 cm of this microwire were annealed (300-600 °C during 1 h). The structural characteristics of the as-cast and annealed samples were determined, at room temperature, by X-ray diffraction (XRD) technique. XRD measurements allow to obtain the evolution of the grain size (15-35 nm) and relative volume fraction (5-60%) of the nanograins as a function of he annealing temperature in the annealed samples. Coercive field (Hc) of the as-cast and annealed samples has been evaluated from the hysteresis loop of the samples obtained by a conventional induction method at 100 Hz. Thermal dependence Hc is quite similar to that reported in other nanocrystalline Fe-based alloys. It slightly decreases from the as-cast state (relaxation process) showing small maximum at around 700 K (pre-nucleation of nanograins) decreasing significantly between 773-873 K (exchange coupling of the nanograins).

Cuvinte-cheie
Devitrification, Magnetic softness, Nanocrystalline alloys, Thin wires

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<title xml:lang='en'>Studies of structural and magnetic properties of glass-coated nanocrystalline Fe79Hf7B12Si2 microwires</title>
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<subject>Devitrification</subject>
<subject>Magnetic softness</subject>
<subject>Nanocrystalline alloys</subject>
<subject>Thin wires</subject>
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