A rapid hydrothermal synthesis of rutile SnO2 nanowires

Lupan Oleg; Chow Lee; Chai Guangyu; Schulte Alfons; Park Sang Hoon; Heinrich Helge H.

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LUPAN, Oleg, CHOW, Lee, CHAI, Guangyu, SCHULTE, Alfons, PARK, Sang Hoon, HEINRICH, Helge H.. A rapid hydrothermal synthesis of rutile SnO2 nanowires. In: Materials Science and Engineering B: Solid-State Materials for Advanced Technology, 2009, vol. 157, p. 0. ISSN 0921-5107. DOI: https://doi.org/10.1016/j.mseb.2008.12.035

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Materials Science and Engineering B: Solid-State Materials for Advanced Technology

Volumul 157 / 2009 / ISSN 0921-5107

A rapid hydrothermal synthesis of rutile SnO₂ nanowires

DOI:https://doi.org/10.1016/j.mseb.2008.12.035

Pag. 0-0

Lupan Oleg¹², Chow Lee¹, Chai Guangyu³, Schulte Alfons¹, Park Sang Hoon¹, Heinrich Helge H.¹

¹ University of Central Florida,
² Technical University of Moldova,
³ Apollo Technologies, Inc.

Disponibil în IBN: 19 iunie 2023

Rezumat

Tin oxide (SnO₂) nanowires with rutile structure have been synthesized by a facile hydrothermal method at 98 °C. The morphologies and structural properties of the as-grown nanowires/nanoneedles were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction, X-ray diffraction and Raman spectroscopy. The SEM images reveal tetragonal nanowires of about 10-100 μm in length and 50-100 nm in radius. The Raman scattering peaks indicate a typical rutile phase of the SnO₂. The effects of molar ratio of SnCl₄ to NH₄OH on the growth mechanism are discussed.

Cuvinte-cheie
hydrothermal synthesis, Nanoneedles, nanowires, tin oxide

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