Conţinutul numărului revistei |
Articolul precedent |
Articolul urmator |
842 17 |
Ultima descărcare din IBN: 2023-05-07 10:11 |
Căutarea după subiecte similare conform CZU |
543.2:615.214.24 (1) |
Metode chimice de analiză (30) |
Medicamentele potrivit acţiunii lor principale (395) |
SM ISO690:2012 ХАРЧУ, И., КАСЬЯН, Игорь, КАСЬЯН, Анна, СИМОНОВА, Л.. Оптимизация подготовки проб для химико-токсикологического анализа барбитуратов методом ВЭЖХ
. In: Revista Farmaceutică a Moldovei , 2014, nr. 1-2, pp. 28-32. ISSN 1812-5077. |
EXPORT metadate: Google Scholar Crossref CERIF DataCite Dublin Core |
Revista Farmaceutică a Moldovei | ||||||
Numărul 1-2 / 2014 / ISSN 1812-5077 | ||||||
|
||||||
CZU: 543.2:615.214.24 | ||||||
Pag. 28-32 | ||||||
|
||||||
Descarcă PDF | ||||||
Rezumat | ||||||
Optimizarea preparării probelor pentru analiza chimico-toxicologică a barbituricilor prin metoda HPLC. In lucrarea dată au fost studiate unele procedee simple de preparare a probelor de material biologic pentru dozarea ulterioară a barbituricilor prin metoda HPLC. Ca procedeu optim se propune deproteinizarea cu amestec metanol – 2 M H2SO4 (95:5). Acest procedeu in ansamblu cu analiza HPLC-UV asigură regăsirea barbituricilor cel puţin 97% din plasma sanguină şi o linearitate inaltă a dependenţei de calibrare in intregul diapazon studiat al concentraţiilor (pană la 160 mg/l) cu limita de cuantificare circa 1 mg/l |
||||||
Cuvinte-cheie Barbiturice, analiza chimico-toxicologică, prepararea probelor, HPLC. |
||||||
|
Cerif XML Export
<?xml version='1.0' encoding='utf-8'?> <CERIF xmlns='urn:xmlns:org:eurocris:cerif-1.5-1' xsi:schemaLocation='urn:xmlns:org:eurocris:cerif-1.5-1 http://www.eurocris.org/Uploads/Web%20pages/CERIF-1.5/CERIF_1.5_1.xsd' xmlns:xsi='http://www.w3.org/2001/XMLSchema-instance' release='1.5' date='2012-10-07' sourceDatabase='Output Profile'> <cfResPubl> <cfResPublId>ibn-ResPubl-40553</cfResPublId> <cfResPublDate>2014-07-01</cfResPublDate> <cfIssue>1-2</cfIssue> <cfStartPage>28</cfStartPage> <cfISSN>1812-5077</cfISSN> <cfURI>https://ibn.idsi.md/ro/vizualizare_articol/40553</cfURI> <cfTitle cfLangCode='RU' cfTrans='o'>Оптимизация подготовки проб для химико-токсикологического анализа барбитуратов методом ВЭЖХ </cfTitle> <cfKeyw cfLangCode='RU' cfTrans='o'>Barbiturice; analiza chimico-toxicologică; prepararea probelor; HPLC.</cfKeyw> <cfAbstr cfLangCode='RO' cfTrans='o'>Optimizarea preparării probelor pentru analiza chimico-toxicologică a barbituricilor prin metoda HPLC. In lucrarea dată au fost studiate unele procedee simple de preparare a probelor de material biologic pentru dozarea ulterioară a barbituricilor prin metoda HPLC. Ca procedeu optim se propune deproteinizarea cu amestec metanol – 2 M H2SO4 (95:5). Acest procedeu in ansamblu cu analiza HPLC-UV asigură regăsirea barbituricilor cel puţin 97% din plasma sanguină şi o linearitate inaltă a dependenţei de calibrare in intregul diapazon studiat al concentraţiilor (pană la 160 mg/l) cu limita de cuantificare circa 1 mg/l</cfAbstr> <cfAbstr cfLangCode='EN' cfTrans='o'>In the present work have been studied some simple procedures of biological material sample preparation for the following assay of barbiturates by the HPLC method. As an optimum way it is offered deproteinization by the mixture of methanol and 2 M H2SO4 (95:5). This procedure in combination with HPLC-UV analysis ensures recovery of barbiturates not less than 97% from blood plasma and high linearity of the calibration dependence in whole investigated range of concentrations (up to 160 mg/l) at limit of quantification about 1 mg/l.. </cfAbstr> <cfResPubl_Class> <cfClassId>eda2d9e9-34c5-11e1-b86c-0800200c9a66</cfClassId> <cfClassSchemeId>759af938-34ae-11e1-b86c-0800200c9a66</cfClassSchemeId> <cfStartDate>2014-07-01T24:00:00</cfStartDate> </cfResPubl_Class> <cfResPubl_Class> <cfClassId>e601872f-4b7e-4d88-929f-7df027b226c9</cfClassId> <cfClassSchemeId>40e90e2f-446d-460a-98e5-5dce57550c48</cfClassSchemeId> <cfStartDate>2014-07-01T24:00:00</cfStartDate> </cfResPubl_Class> <cfPers_ResPubl> <cfPersId>ibn-person-46064</cfPersId> <cfClassId>49815870-1cfe-11e1-8bc2-0800200c9a66</cfClassId> <cfClassSchemeId>b7135ad0-1d00-11e1-8bc2-0800200c9a66</cfClassSchemeId> <cfStartDate>2014-07-01T24:00:00</cfStartDate> </cfPers_ResPubl> <cfPers_ResPubl> <cfPersId>ibn-person-13489</cfPersId> <cfClassId>49815870-1cfe-11e1-8bc2-0800200c9a66</cfClassId> <cfClassSchemeId>b7135ad0-1d00-11e1-8bc2-0800200c9a66</cfClassSchemeId> <cfStartDate>2014-07-01T24:00:00</cfStartDate> </cfPers_ResPubl> <cfPers_ResPubl> <cfPersId>ibn-person-13492</cfPersId> <cfClassId>49815870-1cfe-11e1-8bc2-0800200c9a66</cfClassId> <cfClassSchemeId>b7135ad0-1d00-11e1-8bc2-0800200c9a66</cfClassSchemeId> <cfStartDate>2014-07-01T24:00:00</cfStartDate> </cfPers_ResPubl> <cfPers_ResPubl> <cfPersId>ibn-person-41348</cfPersId> <cfClassId>49815870-1cfe-11e1-8bc2-0800200c9a66</cfClassId> <cfClassSchemeId>b7135ad0-1d00-11e1-8bc2-0800200c9a66</cfClassSchemeId> <cfStartDate>2014-07-01T24:00:00</cfStartDate> </cfPers_ResPubl> </cfResPubl> <cfPers> <cfPersId>ibn-Pers-46064</cfPersId> <cfPersName_Pers> <cfPersNameId>ibn-PersName-46064-1</cfPersNameId> <cfClassId>55f90543-d631-42eb-8d47-d8d9266cbb26</cfClassId> <cfClassSchemeId>7375609d-cfa6-45ce-a803-75de69abe21f</cfClassSchemeId> <cfStartDate>2014-07-01T24:00:00</cfStartDate> <cfFamilyNames>Харчу</cfFamilyNames> <cfFirstNames>И.</cfFirstNames> </cfPersName_Pers> </cfPers> <cfPers> <cfPersId>ibn-Pers-13489</cfPersId> <cfPersName_Pers> <cfPersNameId>ibn-PersName-13489-1</cfPersNameId> <cfClassId>55f90543-d631-42eb-8d47-d8d9266cbb26</cfClassId> <cfClassSchemeId>7375609d-cfa6-45ce-a803-75de69abe21f</cfClassSchemeId> <cfStartDate>2014-07-01T24:00:00</cfStartDate> <cfFamilyNames>Касьян</cfFamilyNames> <cfFirstNames>Игорь</cfFirstNames> </cfPersName_Pers> </cfPers> <cfPers> <cfPersId>ibn-Pers-13492</cfPersId> <cfPersName_Pers> <cfPersNameId>ibn-PersName-13492-1</cfPersNameId> <cfClassId>55f90543-d631-42eb-8d47-d8d9266cbb26</cfClassId> <cfClassSchemeId>7375609d-cfa6-45ce-a803-75de69abe21f</cfClassSchemeId> <cfStartDate>2014-07-01T24:00:00</cfStartDate> <cfFamilyNames>Касьян</cfFamilyNames> <cfFirstNames>Анна</cfFirstNames> </cfPersName_Pers> </cfPers> <cfPers> <cfPersId>ibn-Pers-41348</cfPersId> <cfPersName_Pers> <cfPersNameId>ibn-PersName-41348-1</cfPersNameId> <cfClassId>55f90543-d631-42eb-8d47-d8d9266cbb26</cfClassId> <cfClassSchemeId>7375609d-cfa6-45ce-a803-75de69abe21f</cfClassSchemeId> <cfStartDate>2014-07-01T24:00:00</cfStartDate> <cfFamilyNames>Симонова</cfFamilyNames> <cfFirstNames>Л.</cfFirstNames> </cfPersName_Pers> </cfPers> </CERIF>