Prolonged holding and cyclic loading indentation of aluminophosphate glass: kinetics of deformation
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2021-11-05 10:14
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RĂZLOG (BELEI), Ina, ŞIKIMAKA, Olga, GRABCO, Daria, SAVA, Bogdan Alexandru, BOROICA, Lucica, ELIŞA, Mihail, PYRTSAC, Constantin, PRISĂCARU, Andrian, POPA, Mihail. Prolonged holding and cyclic loading indentation of aluminophosphate glass: kinetics of deformation. In: Materials Science and Condensed Matter Physics, Ed. 8-th Edition, 12-16 septembrie 2016, Chişinău. Chişinău: Institutul de Fizică Aplicată, 2016, Editia 8, p. 185. ISBN 978-9975-9787-1-2.
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Materials Science and Condensed Matter Physics
Editia 8, 2016
Conferința "International Conference on Materials Science and Condensed Matter Physics"
8-th Edition, Chişinău, Moldova, 12-16 septembrie 2016

Prolonged holding and cyclic loading indentation of aluminophosphate glass: kinetics of deformation


Pag. 185-185

Răzlog (Belei) Ina1, Şikimaka Olga1, Grabco Daria1, Sava Bogdan Alexandru2, Boroica Lucica2, Elişa Mihail3, Pyrtsac Constantin1, Prisăcaru Andrian1, Popa Mihail1
 
1 Institute of Applied Physics, Academy of Sciences of Moldova,
2 National Institute for Laser, Plasma and Radiation Physics (INFLPR),
3 National Institute for Optoelectronics INOE2000, Magurele
 
 
Disponibil în IBN: 30 iulie 2019


Rezumat

The time-dependent mechanical behavior of aluminophosphate glasses (APG) (Li2O–Al2O3–BaO– La2O3–P2O5–RE2O3, RE = Dy, Tb) subjected to dynamic indentation under prolonged holding and cyclic loading conditions in combination with different loading rates is presented in this work. Analysis of the load-displacement (P-h) and displacement-time (h-t) dependences was applied to investigate the deformation peculiarities and kinetics of deformation in these conditions.   The 300 s holding under the maximum load during indentation shows a creep of material (continued deformation under constant peak load, Pmax) (Fig. 1, a), which appears to be dependent on the loading rate and namely, the higher the loading rate, the larger the total displacement during creep (Fig. 1, b). For both types of indentation made with high and low loading rates, the creep rate (dh/dt) has a decelerating character at the beginning of the creep portion setting to a constant value after 50-100 s and this value is higher for higher loading rate indentation (20 mN/s). The application of different loading rate may cause the modification of the relative contribution of certain deformation mechanisms specific to phosphate glasses, such as, permanent densification, plastic flow and fracture [1], which in turn can cause different deformation behavior.   The applied cyclic indentation, prolonged holding indentation (Fig. 1, a) and a combination of them (Fig. 1, c) represents in fact a modeling of wear and fatigue processes. The using of these loading conditions leads to the decrease of hardness values in comparison with those obtained under standard indentation conditions with short holding time (5 s) and one loading-unloading cycle. The cyclic indentation combined with holding showed the maximum hardness decrease of 32% and 17% for APG-Dy and APG-Tb, respectively, for loading rate of 2 mN/s. For 20 mN/s rate these values are somewhat smaller, 22 and 14%, respectively. The cyclic indentation induces the smallest decrease of hardness and the indentation with prolonged holding has intermediate position. This tendency is maintained for both glasses and both loading rates used. These results suggest about the time dependence of the deformation processes in APG resulting in a loss of material strength