Synthesis and X-ray analysis of new tetranorlabdane compound with thiodiazole unit

Lungu Lidia; Vicol Crina; Aricu Aculina; Ciocarlan Alexandru; Barba Alic; Shova Sergiu

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2023-05-13 08:30

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LUNGU, Lidia, VICOL, Crina, ARICU, Aculina, CIOCARLAN, Alexandru, BARBA, Alic, SHOVA, Sergiu. Synthesis and X-ray analysis of new tetranorlabdane compound with thiodiazole unit. In: Materials Science and Condensed Matter Physics, Ed. 8-th Edition, 12-16 septembrie 2016, Chişinău. Chişinău: Institutul de Fizică Aplicată, 2016, Editia 8, p. 155. ISBN 978-9975-9787-1-2.

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Materials Science and Condensed Matter Physics
Editia 8, 2016

Conferința "International Conference on Materials Science and Condensed Matter Physics"
8-th Edition, Chişinău, Moldova, 12-16 septembrie 2016

Synthesis and X-ray analysis of new tetranorlabdane compound with thiodiazole unit

Pag. 155-155

Lungu Lidia, Vicol Crina, Aricu Aculina, Ciocarlan Alexandru, Barba Alic, Shova Sergiu

Institute of Chemistry of the Academy of Sciences of Moldova

Disponibil în IBN: 29 iulie 2019

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The three steps synthesis of tetranorlabdane compound 2 containing thiadiazole unit was performed starting from commercially available norambreinolide 1 with an overall yield of 76% (scheme 1). The structure of compound 2 was established on the basis of their 1H and 13C NMR data. OH O N S N S O 1 O 2 3 steps Crystal structures of original tetranorlabdane derivative with thiadiazole unit 2 have been studied by single-crystal X-ray diffraction (Fig. 1). According to this metod compound 2 crystalize in P212121 space group of orthorhombic system. The crystal structure of the title compound includes the molecules 2 and doesn’t contain any solvate molecules.

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