Micro- and macro-mechanical properties of aluminophosphate glasses depending on their compozition and loading conditions
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SHIKIMAKA, Olga A., GRABCO, Daria, SAVA, Bogdan Alexandru, ELIŞA, Mihail, BOROICA, Lucica, HAREA, Evghenii, PYRTSAC, Constantin, PRISĂCARU, Andrian, SPOIALĂ, Dorin. Micro- and macro-mechanical properties of aluminophosphate glasses depending on their compozition and loading conditions. In: Materials Science and Condensed Matter Physics, Ed. 7, 16-19 septembrie 2014, Chișinău. Chișinău, Republica Moldova: Institutul de Fizică Aplicată, 2014, Editia 7, p. 131.
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Materials Science and Condensed Matter Physics
Editia 7, 2014
Conferința "Materials Science and Condensed Matter Physics"
7, Chișinău, Moldova, 16-19 septembrie 2014

Micro- and macro-mechanical properties of aluminophosphate glasses depending on their compozition and loading conditions


Pag. 131-131

Shikimaka Olga A.1, Grabco Daria1, Sava Bogdan Alexandru2, Elişa Mihail3, Boroica Lucica2, Harea Evghenii1, Pyrtsac Constantin1, Prisăcaru Andrian1, Spoială Dorin4
 
1 Institute of Applied Physics, Academy of Sciences of Moldova,
2 National Institute for Laser, Plasma and Radiation Physics (INFLPR),
3 Institute of Optoelectronics Bucarest-Magurele,
4 Moldova State University
 
Disponibil în IBN: 4 martie 2019


Rezumat

In this study the deformation peculiarities of aluminophosphate glasses (Li2O-Al2O3-BaO-La2O3- P2O5) doped with Dy, Tb and Fe were investigated at concentated load action (indentation) and uniaxial compression. Dynamic nanoindentation techique with Berkovich indenter were used for hardness (H) and elastic modulus (E) measurements, as well as for the investigation of the kinetics of deformation through the analisys of strain rate during indentation and its influence on the deformation mechanisms. It is known that there are two main mechanisms responsible for the plastic deformation of glassy matrix: particular modes of shear flow and permanent densification. The contribution of densification influenced by strain rate under indentation was studied by using thermally-induced indentation recovery that takes place mainly at the expense of densification. It was shown that the decrease of load and loading (strain) rate leads to the increase of densification contribution to the total process of deformation under indentation (Fig.1). The influence of loading rate on hardness is not so pronounced although some growth of hardness with rate increase was observed.  The strain rate appears to be responsible for different behavior during uniaxial compression (macroscale) as well, that becomes apparent by higher ultimate strength and strain that the material can withstand during longer period of time before disruption when the deformation occur at slower rate. This is consistent with the results obtained under concentated load action (micro-scale). By using quasistatic Vickers microindentation method the fracture toughness evaluation were performed. The addition and change of doping element does not affect essentially the fracture resistance, the values ranging from 0.79 to 0.83 MPa·m1/2. As for hardness, it was observed an increase with the addition of Fe and Dy and a small decrease with the addition of Tb, the values ranging from 5.54 to 6.25 GPa for 100 mN load. These are rather good parameters that testify to good homogeneity and low defect structure of glasses due to the application of non-conventional wet chemical raw materials processing technique for their fabrication.