Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde
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PULYA, A. V.; SEIFULLINA, Inna; SKOROKHOD, L. S.; PAVLOVSKY, Victor; KRAVTSOV, Viktor; BOGZA, Sergei L.; SUIKOV, Su Yu. Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde. In: Journal of Structural Chemistry. 2018, nr. 2(59), pp. 497-501. ISSN 0022-4766.
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Journal of Structural Chemistry
Numărul 2(59) / 2018 / ISSN 0022-4766

Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde


DOI: 10.1134/S002247661802035X
Pag. 497-501

Pulya A. V.1, Seifullina Inna2, Skorokhod L. S.1, Pavlovsky Victor3, Kravtsov Viktor4, Bogza Sergei L.5, Suikov Su Yu5
 
1 Odessa National I.I Mechnikov University,
2 Odessa I.I.Mechnikov National University, Odessa,
3 A.V. Bogatsky Physico-Chemical Institute of the NAS of Ukraine,
4 Institute of Applied Physics, Academy of Sciences of Moldova,
5 L. M. Litvinenko Institute of Physical-Organic Chemistry and Coal Chemistry
 
Disponibil în IBN: 21 iunie 2018


Rezumat

Hydrazone [HydrHSal]∙Н2О is synthesized for the first time by the interaction of 2-(7-bromo-2-oxo-5- phenyl-3H-1,4-benzdiazepin-1-yl)acetohydrazide (gidazepam) with salicylic aldehyde and characterized by the elemental analysis, thermogravimetry, mass, electron, IR, and NMR spectroscopic techniques. The molecular and crystal structure is determined by single crystal X-ray diffraction.

Cuvinte-cheie
2-(7-bromo-2-oxo-5-phenyl-3H-1,4-benzdiazepin-1-yl)acetohydrazide, gidazepam, hydrazone, molecular structure, salicylic aldehyde, single crystal X-ray diffraction analysis