Synthesis and structural characteristics of BIS(Citrate)Germanates(IV) (Hbipy)2 [Ge(HCit)2]•2H2O AND [CuCl(bipy)2] 2[Ge(HCit) 2]•8H2O

Seifullina Inna; Martsinko Elena; Chebanenko Elena; Pirozhok Olha; Dyakonenko Viktoriya; Shishkina Svitlana

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SEIFULLINA, Inna, MARTSINKO, Elena, CHEBANENKO, Elena, PIROZHOK, Olha, DYAKONENKO, Viktoriya, SHISHKINA, Svitlana. Synthesis and structural characteristics of BIS(Citrate)Germanates(IV) (Hbipy)2 [Ge(HCit)2]•2H2O AND [CuCl(bipy)2] 2[Ge(HCit) 2]•8H2O. In: Chemistry Journal of Moldova, 2016, nr. 2(11), pp. 52-57. ISSN 1857-1727. DOI: https://doi.org/10.19261/cjm.2016.11(2).11

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Chemistry Journal of Moldova

Numărul 2(11) / 2016 / ISSN 1857-1727 /ISSNe 2345-1688

Synthesis and structural characteristics of BIS(Citrate)Germanates(IV) (Hbipy)2 [Ge(HCit)2]•2H2O AND [CuCl(bipy)2] 2[Ge(HCit) 2]•8H2O

DOI:https://doi.org/10.19261/cjm.2016.11(2).11

CZU: 543.8+543.5

Pag. 52-57

Seifullina Inna¹, Martsinko Elena¹, Chebanenko Elena¹, Pirozhok Olha¹, Dyakonenko Viktoriya², Shishkina Svitlana³²

¹ Odesa I.I.Mechnikov National University,
² Institute for Single Crystals of NAS of Ukraine,
³ V.N.Karazin Kharkiv Natsonal University

Proiecte:

INTAS Optimisation of Tartaric acid and enonotanines extraction from winery wastes and their utilization for the synthesis of new compounds with biological activity and antioxidant properties

Disponibil în IBN: 26 decembrie 2016

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The crystalline compounds (Hbipy)2[Ge(HCit)2]·2H2O (1) and [CuCl(bipy)2]2[Ge(HCit)2]·8H2O (2) (where H4Cit is citric acid, bipy is 2,2ʹ-bipyridine) were obtained for the fi rst time and their structures were determined by the single-crystal X-ray diffraction method. Compounds were characterized by IR spectroscopy, thermogravimetric (TGA) and elemental analyses. Both compounds are formed with complex bis(citrate)germanate anion and protonated 2,2’-bipyridine or [Cu(bipy)2Cl] as cations in compounds 1 and 2, respectively.

Cuvinte-cheie
germanium(IV) compound, 2’- bipyridine,

citric acid, 2, copper(II) complex, structure