Conţinutul numărului revistei |
Articolul precedent |
Articolul urmator |
194 0 |
Căutarea după subiecte similare conform CZU |
547.7/.8:54.057 (1) |
Chimie organică (484) |
Obținere. Preparare. Izolare. Purificare etc. (51) |
SM ISO690:2012 RAJENDRA, Patil, CHAVAN, Jagdish, PATEL, Shivnath, BELDAR, Anil, SHINDE, Vaishali. Mild acidic charcoal catalyzed synthesis of 3,4-dihydropyrimidin-2(1H)-one/-thione derivatives. In: Chemistry Journal of Moldova, 2022, nr. 2(17), pp. 101-108. ISSN 1857-1727. DOI: https://doi.org/10.19261/cjm.2022.999 |
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Chemistry Journal of Moldova | ||||||
Numărul 2(17) / 2022 / ISSN 1857-1727 /ISSNe 2345-1688 | ||||||
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DOI:https://doi.org/10.19261/cjm.2022.999 | ||||||
CZU: 547.7/.8:54.057 | ||||||
Pag. 101-108 | ||||||
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Abstract. A mild catalyst system with comparative reduction in amount of catalyst was demonstrated. The multicomponent synthesis of 3,4-dihydropyrimidin-2(1H)-ones and -thiones using acetic acid supported on activated charcoal as a mild acid catalyst in ethanol under both conventional as well as microwave irradiation conditions has been achieved. The obtained catalyst system is more efficient under microwave irradiation than under conventional conditions with shorter reaction times (3-9 min) and excellent yields (78-94 %). |
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Cuvinte-cheie Biginelli reaction, acetic acid, acidic charcoal, microwave irradiation |
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