Hydrothermal and Electrochemical Synthesis of MoS2 Nanoparticles and Characterization of the Latter
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LASCOVA-BACIU, Renata. Hydrothermal and Electrochemical Synthesis of MoS2 Nanoparticles and Characterization of the Latter. In: Surface Engineering and Applied Electrochemistry, 2020, nr. 2(56), pp. 127-132. ISSN 1068-3755. DOI: https://doi.org/10.3103/S1068375520020118
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Surface Engineering and Applied Electrochemistry
Numărul 2(56) / 2020 / ISSN 1068-3755 /ISSNe 1934-8002

Hydrothermal and Electrochemical Synthesis of MoS2 Nanoparticles and Characterization of the Latter

DOI:https://doi.org/10.3103/S1068375520020118

Pag. 127-132

Lascova-Baciu Renata
 
Institute of Applied Physics
 
 
Disponibil în IBN: 16 octombrie 2020


Rezumat

The characteristic features of the hydrothermal synthesis of molybdenum sulfide nanoparticles, using Na2MoO4 as the molybdenum precursor and thioacetamide as the sulfur precursor, at a synthesis temperature of 220°C, and of electrochemical synthesis—anodic formation of nanoparticles from MoS2 single crystals by electrolysis in an ionic liquid—are described. The X-ray fluorescence, optical absorption, and photoluminescence spectroscopy methods were applied for characterization of the nanoparticles produced. 

Cuvinte-cheie
hydrothermal synthesis, ionic liquids, layered semiconductors, Light absorption, Molybdenum compounds, nanoparticles, Photoluminescence spectroscopy, Sodium compounds, Spectroscopic analysis