Articolul precedent |
Articolul urmator |
486 2 |
Ultima descărcare din IBN: 2022-12-06 11:18 |
SM ISO690:2012 MEZEY, Reka-Stefana, PAKHONTSU, E., ILIES, D., SHOVA, Sergiu, GULYA, Aurelian, ROSHU, T.. Synthesis, structural and spectral studies of Cu(II) and V(IV) complexes of a novel Schiff base derived from pyridoxal. Antimicrobial activity. In: Physical Methods in Coordination and Supramolecular Chemistry, 24-26 octombrie 2012, Chişinău. Chisinau, Republic of Moldova: 2012, XVII, p. 111. |
EXPORT metadate: Google Scholar Crossref CERIF DataCite Dublin Core |
Physical Methods in Coordination and Supramolecular Chemistry XVII, 2012 |
||||||
Conferința ""Physical Methods in Coordination and Supramolecular Chemistry"" Chişinău, Moldova, 24-26 octombrie 2012 | ||||||
|
||||||
Pag. 111-111 | ||||||
|
||||||
Descarcă PDF | ||||||
Rezumat | ||||||
A novel Schiff base, N-(4-amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-one) pyridoxaldimine (HL·HCl), was prepared and structurally characterized on the basis of elemental analyses, 1H NMR, 13C NMR and IR spectral data. The synthesis and characterization of several Cu(II) (1–6) and V(IV) (7) complexes with N-(4-amino-2,3- dimethyl-1-phenyl-3-pyrazolin-5-one)pyridoxaldimine are reported.fgiureFig. 1 Structure of [CuHL(H2O)2] + cation in 1 The composition and structures of the copper(II) and vanadium(IV) complexeswere proposed based on elemental analyses, molar conductance, magnetic susceptibility measurements, IR, electronic and EPR spectroscopy. In addition, the structures of the ligand and the complex [CuL(H2O)2]NO3·2.25H2O (1) have been determined by single-crystal X-ray diffraction, showing that the Cu(II) center has a distorted square-pyramidal geometry. The ligand and the complexes were also tested for their in vitro antibacterial activity. |
||||||
|
Crossref XML Export
<?xml version='1.0' encoding='utf-8'?> <doi_batch version='4.3.7' xmlns='http://www.crossref.org/schema/4.3.7' xmlns:xsi='http://www.w3.org/2001/XMLSchema-instance' xsi:schemaLocation='http://www.crossref.org/schema/4.3.7 http://www.crossref.org/schema/deposit/crossref4.3.7.xsd'> <head> <doi_batch_id>ibn-104621</doi_batch_id> <timestamp>1713569760</timestamp> <depositor> <depositor_name>Information Society Development Instiute, Republic of Moldova</depositor_name> <email_address>idsi@asm.md</email_address> </depositor> </head> <body> <collection> <collection_metadata> <full_title>Physical Methods in Coordination and Supramolecular Chemistry</full_title> </collection_metadata> <collection_issue> <publication_date media_type='print'> <year>2012</year> </publication_date> </collection_issue> <collection_article publication_type='full_text'><titles> <title>Synthesis, structural and spectral studies of Cu(II) and V(IV) complexes of a novel Schiff base derived from pyridoxal. Antimicrobial activity</title> </titles> <contributors> <person_name sequence='first' contributor_role='author'> <given_name>Reka-Ștefana</given_name> <surname>Mezey</surname> </person_name> <person_name sequence='additional' contributor_role='author'> <given_name>Elena Mihaela</given_name> <surname>Pahontu</surname> </person_name> <person_name sequence='additional' contributor_role='author'> <given_name>Diana-Carolina</given_name> <surname>Ilies</surname> </person_name> <person_name sequence='additional' contributor_role='author'> <given_name>Sergiu</given_name> <surname>Şova</surname> </person_name> <person_name sequence='additional' contributor_role='author'> <given_name>Aurelian</given_name> <surname>Gulea</surname> </person_name> <person_name sequence='additional' contributor_role='author'> <given_name>Tudor</given_name> <surname>Roşu</surname> </person_name> </contributors> <publication_date media_type='print'> <year>2012</year> </publication_date> <pages> <first_page>111</first_page> <last_page>111</last_page> </pages> </collection_article> </collection> </body> </doi_batch>